The samples were examined with a Philips CM 100 TEM (Philips, Eindhoven, The Netherlands) operated at an accelerating voltage of 80 kV and equipped with a SIS MegaView2 or an OSIS Veleta digital slow scan 2 k 2 k CCD camera. Digital images were recorded with the analySIS or ITEM software packages and further processed using Adobe Photoshop software (Adobe Systems Incorporated, San Jose, California, CA, USA) to enhance contrast and brightness.
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